2023 Vol. 44, No. 5

Mining & Beneficiation
Optimization of flotation process of ilmenite based on Box-Behnken response surface methodology
Dai Chuan, Chen Pan, Sun Wei, Wang Hongbin, Yang Yaohui
2023, 44(5): 1-7. doi: 10.7513/j.issn.1004-7638.2023.05.001
Abstract(268) HTML (80) PDF(28)
Abstract:
In order to address the complex challenge of ilmenite flotation separation, an extensive single-factor variable test was conducted to investigate the parameters influencing ilmenite flotation and determine the optimal process conditions. To gain a comprehensive understanding of the parameter interac...
Flotation dynamics test and analysis for ilmenite
Ma Chonghan, Fan Xuesai, Chen Feifei
2023, 44(5): 8-14. doi: 10.7513/j.issn.1004-7638.2023.05.002
Abstract(297) HTML (54) PDF(13)
Abstract:
Magnetic separation plus flotation has gradually become the best process for comprehensive recovery of ilmenite. Flotation recovery is faced with the characteristics of large specific ore, coarse particle size, high slurry concentration (ca. 65%), and high mass pull. According to the existing flotat...
Study on the comprehensive recovery of Fe and Ti from a low grade vanadium-titanium magnetite in Xinjiang
Ma Donglin, Yang Yaohui, Deng Jian, Yan Weiping, Wang Hongbin
2023, 44(5): 15-22. doi: 10.7513/j.issn.1004-7638.2023.05.003
Abstract(307) HTML (62) PDF(36)
Abstract:
Aiming at a low-grade vanadium titanomagnetite resource in Xinjiang, an experimental study on efficient comprehensive recovery of iron and titanium benefication was carried out. According to the specific properties of the ore, a technological process of iron and titanium comprehensive recovery was d...
Differences between oleic acid and benzohydroxamic acid in flotation performance of ilmenite
Yang Zhaojun, Xie Baohua, Liang Taomao, Wang Fengyu, Zhong Senlin
2023, 44(5): 23-27. doi: 10.7513/j.issn.1004-7638.2023.05.004
Abstract(244) HTML (51) PDF(10)
Abstract:
Starting from the study of interface properties of ilmenite, the single mineral flotation test, collector adsorption capacity, contact angle, and ζ potential measurement were conducted to study the mechanism of oleic acid and benzohydroxamic acid on the flotation of ilmenite. Oleic acid and benzohyd...
Experimental study on beneficiation of a low-grade refractory iron ore in Qinghai province
Luo Yunbo, Xiao Jinxiong, Shi Yunliang, Xie Baohua
2023, 44(5): 28-35. doi: 10.7513/j.issn.1004-7638.2023.05.005
Abstract(214) HTML (66) PDF(10)
Abstract:
Aiming at the characteristics of low iron grade, fine distribution size of magnetite and complex relationship with gangue minerals of a refractory iron ore in Qinghai province, the technological process of dry throw-stage grinding and stage magnetic separation was adopted for experimental study. The...
Experimental study on beneficiation of a foreign refractory ilmenite ore
Xie Baohua, Luo Yunbo, Wang Fengyu, Liang Taomao, Yang Zhaojun
2023, 44(5): 36-40. doi: 10.7513/j.issn.1004-7638.2023.05.006
Abstract(231) HTML (42) PDF(18)
Abstract:
In view of the complex mineral composition of a ilmenite from overseas, the close symbiotic relationship between valuable minerals and the fine particle size of ilmenite, the experimental study on the beneficiation process of the refractory ilmenite ore was carried out using the stage grinding-stage...
Optimization of stope structure parameters based on Mathews and FLAC3D
Li Cui, Zhang Liangbing, Chen Tao, Luo Shaochen
2023, 44(5): 41-47. doi: 10.7513/j.issn.1004-7638.2023.05.007
Abstract(338) HTML (110) PDF(11)
Abstract:
Taking an underground mine in Panxi as an example, the exposed area of the stope was estimated based on Mathews stability diagram method and empirical analogy method. It is recommended that the allowable exposed area of the stope roof is 800 to 1200 square meters, and the allowable exposed area of t...
Analysis and research on cover thickness of non-pillar sublevel caving method in an iron mine in Panxi
Zhang Liangbing, Leng Jianyong, Li Cui, Chen Tao, Luo Shaochen
2023, 44(5): 48-52. doi: 10.7513/j.issn.1004-7638.2023.05.008
Abstract(251) HTML (113) PDF(14)
Abstract:
Aiming at solving the problem of determining the reasonable thickness of the overburden layer in the conversion of open-pit to underground caving mining of the hanging wall ore body in an iron mine in Panxi, the Similarity Model test and Numerical Simulation were used to analyze and study the moveme...
Application of Vanadium and Titanium
Thermodynamic analysis of the effect of oxygenation on the low-temperature chlorination selectivity of carbonized slag
Yue Dong, Wen Liangying, Chen Rong, Wang Jianxin, Yang Yangjun
2023, 44(5): 53-60. doi: 10.7513/j.issn.1004-7638.2023.05.009
Abstract(270) HTML (88) PDF(31)
Abstract:
Based on the Factsage thermodynamic software and database, the effects of introducing oxygen on the TiC and calcium magnesium oxide chlorination in titanium carbide slag are analyzed, and the regulatory scheme of adding oxygen to selectively enhance the chlorination reaction of TiC in the slag while...
Study on thermal deformation behavior and microstructure evolution of Ti-55511 alloy
Mu Pengwei, Lü Shufeng, Yang Peijie, Kang Xudong, Du Zhaoxin
2023, 44(5): 61-67. doi: 10.7513/j.issn.1004-7638.2023.05.010
Abstract(204) HTML (122) PDF(18)
Abstract:
The thermal deformation behavior of Ti-55511 alloy was studied by isothermal compression simulation method at the temperature of 700~950 ℃ and strain rate of 0.001~10 s−1. The results show that the softening mechanism of the alloy is very sensitive to the change of hot working parameters. Under the ...
Effect of post heat treatment on the microstructure and properties of as-annealed Ti75 alloy
Yin Yanchao, Li Longteng, Lü Yifan, Sun Zhijie, Yu Wei, Jiang Peng
2023, 44(5): 68-75. doi: 10.7513/j.issn.1004-7638.2023.05.011
Abstract(235) HTML (69) PDF(24)
Abstract:
In order to study the effect of post heat treatment on the properties of annealed Ti75 alloy, different post treatment conditions including annealing temperatures and cooling rates were selected to treat the annealed Ti75 alloy. The microstructure evolution was analyzed by OM and SEM, and the influe...
Numerical simulation of the effect of post-welding heat treatment on fatigue life of titanium alloy butt plate
Luo Jiayuan, Zhang Yuxiang, Lü Chenke
2023, 44(5): 76-83. doi: 10.7513/j.issn.1004-7638.2023.05.012
Abstract(233) HTML (98) PDF(12)
Abstract:
Based on the finite element software, a thermo-elastic-plastic finite element model of 30 mm thick TC4 titanium alloy butt plate considering the creep stress relaxation effect was established. The temperature field and stress field in the electron beam welding process of TC4 titanium alloy butt plat...
Study on wear resistance of nitriding coatings of Ti-Al base multielement alloys
Zhang Qian, Ma Lan, Yang Shaoli, Zhu Kuisong
2023, 44(5): 84-92. doi: 10.7513/j.issn.1004-7638.2023.05.013
Abstract(163) HTML (82) PDF(10)
Abstract:
In this paper, the titanium-aluminum-based multi-component alloy was prepared from Panzhihua acid-soluble titanium slag, aluminum powder and calcium oxide. After directly nitriding treatment at different temperatures and different time, a nitrided layer was obtained. Scanning electron microscopy, X-...
Study on surface coating modification of silicon anode material with titanium dioxide
Wang Shiwei, Zheng Hao, Meng Weiwei
2023, 44(5): 93-97. doi: 10.7513/j.issn.1004-7638.2023.05.014
Abstract(345) HTML (77) PDF(28)
Abstract:
Titanium dioxide coated silicon (Si@TiO2) nanocomposites with core-shell structure was prepared by hydrolysis method using TiCl4 as titanium source and commercial nano-Si as silicon source. The materials were characterized and tested by XRD, SEM, TEM and electrochemical platform. The results show th...
Resources Environment and Energy Saving
A new low carbon high value route for hydrogen reduction of zinc containing dust
Teng Fei, Guo Peimin, Zhu Deqing, Long Hongming, Li Kai, Wang Lei, Kong Lingbing
2023, 44(5): 98-104. doi: 10.7513/j.issn.1004-7638.2023.05.015
Abstract(221) HTML (67) PDF(18)
Abstract:
In this paper, the theory and technology of comprehensive utilization of zinc containing dust in steel plants at home and abroad are analyzed. The pyrometallurgical process is based on high-temperature carbon metallurgy with coal carrier. High energy consumption, enlarged carbon emission and serious...
Experimental study on quality improvement and impurity reduction of a vanadium-titanium iron concentrate in Panxi
Li Shuo, Chen Fulin, Cai Xianyan, Huang Liyu, Wang Zhijie, Wu Ning, Huang Yan
2023, 44(5): 105-110. doi: 10.7513/j.issn.1004-7638.2023.05.016
Abstract(216) HTML (52) PDF(16)
Abstract:
The TFe grade of a vanadium-titanium-iron concentrate in Panxi is 55.88%. The chemical composition of the main impurity elements in the sample include TiO2, SiO2, Al2O3, MgO and CaO, the proportion of impurities such as granular ilmenite and gangue minerals accountes for 14.26%. Ilmenite is mainly e...
Experimental study on phosphorus flotation of an iron tailings in northern China
Rong Yiyang, Ye Guohua, Kang Xuanxiong, Zhu Siqin, Song Changxu, Xiang Xinyue, Zhang Yun
2023, 44(5): 111-115. doi: 10.7513/j.issn.1004-7638.2023.05.017
Abstract(220) HTML (72) PDF(11)
Abstract:
An iron tailings in the northern China contains 2.93% P2O5, most of which is crystalline apatite and belongs to low-grade phosphorus resources. In order to realize the efficient recovery of phosphorus in the iron tailings, the experimental study on phosphorus flotation was carried out according to i...
Study on concentration process of titanium white waste acid by sulfuric acid method
Wang Haibo, Sun Ke
2023, 44(5): 116-121. doi: 10.7513/j.issn.1004-7638.2023.05.018
Abstract(299) HTML (104) PDF(22)
Abstract:
In order to improve the efficiency of waste acid concentration, the single factor test and orthogonal test of waste acid concentration process were carried out in the laboratory by using vacuum rotary evaporator to simulate the vacuum evaporation concentration of waste acid. Then, based on the resul...
Ferrous Metallurgy and Materials
Evolution characteristics of cavitation bubble size in liquid steel under power ultrasound
Wang Shun, Chen Min, Guo Qing, Cheng Weihao
2023, 44(5): 122-129. doi: 10.7513/j.issn.1004-7638.2023.05.019
Abstract(221) HTML (66) PDF(13)
Abstract:
The effects of sound pressure amplitude, frequency, initial equilibrium radius of the cavitation bubble and gas multiplicity index on the cavitation bubble size in the liquid steel were investigated by solving the function of the power ultrasonic action period T and the cavitation bubble radius R us...
Effect of vanadium content on microstructure and strength plasticity of X80 pipeline steel
Li Longfei, Lin Tengchang, Meng Huadong, Zhang Yang
2023, 44(5): 130-138. doi: 10.7513/j.issn.1004-7638.2023.05.020
Abstract(218) HTML (59) PDF(23)
Abstract:
In this work, the precipitates and microstructure characteristics in four X80 pipeline steels with different vanadium contents (0.036%, 0.075%, 0.110% and 0.150%) and their effects on the strength and plasticity of the steels were investigated by means of high-resolution transmission electron micros...
Study on solid solution behavior of second phase particles and austenite grain growth law of Nb-Ti high strength steel
Yang Jianwei, Yang Qin, Wu Jing, Zheng Yaxu, Wang Yunhui
2023, 44(5): 139-145. doi: 10.7513/j.issn.1004-7638.2023.05.021
Abstract(316) HTML (135) PDF(21)
Abstract:
The solid solution behavior of nanocarbide and austenite grain growth in Nb-Ti microalloyed steel during high temperature heating were studied by means of transmission electron microscope, optical microscope and thermodynamic calculation. The results show that the austenite grain size and size of pr...
Bainite design in quenching and partitioning steel based on numerical calculation
Wu Meng, Hu Zhiping, Liu Rendong, Lin Chunqing, Gu Xingli, Xu Xin
2023, 44(5): 146-150. doi: 10.7513/j.issn.1004-7638.2023.05.022
Abstract(167) HTML (71) PDF(12)
Abstract:
In this study, an optimum design of bainite phase in the commercial quenching and partitioning (Q&P) steel was achieved through the combined results from thermodynamics, kinetics analysis and the pilot experiments. Considering the complex microstructure evolution during partitioning stage of the...
Effect of Cr content on the austenitization of 500 MPa class high-strength seismic rebars
Wang Wentao, Liu Xing, Cao Jianchun, Chen Wei, Yin Shubiao
2023, 44(5): 151-157. doi: 10.7513/j.issn.1004-7638.2023.05.023
Abstract(171) HTML (58) PDF(15)
Abstract:
The microstructure was observed by means of optical microscope, scanning electron microscope, etc. The change of austenite grains of the steels with different Cr contents under different reheating temperature and holding time of the casting billet was studied. The effect of Cr content on austenitiza...
Rheological behaviours and constitutive models of 9Cr18Mo stainless steel at high temperature and high strain rate
Jia Haishen, Shen Jiancheng, Luo Wencui, Yi Xiangbin
2023, 44(5): 158-166. doi: 10.7513/j.issn.1004-7638.2023.05.024
Abstract(247) HTML (60) PDF(13)
Abstract:
The compression tests of 9Cr18Mo stainless steel were conducted by using the UTM5305 universal testing machine and the split Hopkinson pressure bar (SHPB) test device. In this way, the stress–strain curves pertaining to quasi-static (strain rate: 0.001-0.1 s−1) and dynamic (temperature: 25-650 ℃ and...
Study on the hot ductility of titanium microalloyed high-strength beam steels
Song Yu, Gao Zhijun, Wang Shuize, Yin Jingjing
2023, 44(5): 167-175. doi: 10.7513/j.issn.1004-7638.2023.05.025
Abstract(274) HTML (94) PDF(18)
Abstract:
High-temperature tensile tests have been conducted to examine the thermoplasticity of titanium microalloyed high-strength beam steels in the temperature range of 600 ℃ to 1300 ℃. Thermo-calc, the thermodynamic calculation software, was used to calculate the main precipitation intervals in various ex...
Effect of on-line solution treatment on the microstructure and mechanical properties of 2507 duplex stainless steels
Xu Haijian, Han Chufei, Guo Cheng, Qiao Xin, Liu Liu, Sha Xiaochun
2023, 44(5): 176-179. doi: 10.7513/j.issn.1004-7638.2023.05.026
Abstract(244) HTML (66) PDF(12)
Abstract:
Effects of on-line solution treatment and holding time on the microstructure and mechanical properties of 2507 duplex stainless steels were studied by hot-rolling experiments, Zeiss optical microscope (OM) and transmission electron microscopy (TEM). The results show that the volume fraction of ferri...
Analysis on the formation of V-shape segregation in rail steel bloom
Li Hongguang, Xu Mingli, Feng Yuanchao, Zeng Wu
2023, 44(5): 180-187. doi: 10.7513/j.issn.1004-7638.2023.05.027
Abstract(244) HTML (61) PDF(20)
Abstract:
In order to improve V-shape segregation in rail steel bloom, the feature of macro-profile and microstructure were tested and theoretical shrinkage value and actual volume of V-shape was compared. The influencing factors including dynamic soft reduction processes, grade of steel and technology of mic...
Processing parameters, microstructures and mechanical property of Al/steel dissimilar metals butt joint made by CMT welding-brazing
Yu Tengyi, Li Wei, Yu Gaoyang, Li Yan, Chen Shuhai, Liu Ke
2023, 44(5): 188-194. doi: 10.7513/j.issn.1004-7638.2023.05.028
Abstract(283) HTML (55) PDF(11)
Abstract:
A 2 mm thick Q235 steel plate and a 5052 aluminum alloy plate had been used for CMT arc butt welding-brazing. The effects of welding speed and wire feeding speed on joint weld formation, interface microstructure and mechanical properties were studied. The results show that when the wire feeding spee...
Study on the inheritance relationship between billet and rail surface defects
Tao Gongming, Zhu Jun, Deng Feng, Sun Jin
2023, 44(5): 195-200. doi: 10.7513/j.issn.1004-7638.2023.05.029
Abstract(256) HTML (90) PDF(10)
Abstract:
In the test, artificial defects were made in the rolling slip area and rolling stable area on the surface of the casting slab without over standard defects. Normal heating, rolling and straightening processes were adopted, and samples were taken and polished at the corresponding artificial defects o...
Analysis of standard GB/T 3623-2022: titanium and titanium alloy wire
Xie Chen, Wei Jiaqi, Zhang Wei, Feng Yongqi, Feng Junning, Ma Zhongxian, Hu Zhijie, Tao Hailin
2023, 44(5): 201-204. doi: 10.7513/j.issn.1004-7638.2023.05.030
Abstract(825) HTML (417) PDF(34)
Abstract:
This article mainly introduced the revision background, historical evolution, and standard analysis of the new standard GB/T 3623-2022. This article is in order to provide guidance for the reference, production and acceptance of the standard in the follow-up process, deepen the understanding of the ...