2020 Vol. 41, No. 4

Separating and Extracting of Vanadium and Titanium
Simultaneous Extraction of Vanadium and Chromium from Vanadium-chromium Slag by Sodium Roasting
Fu Zibi, Jiang Lin, Li Ming, Wu Zhenxiu
2020, 41(4): 1-6. doi: 10.7513/j.issn.1004-7638.2020.04.001
Abstract(154) PDF(12)
Abstract:
Based on the theoretical analysis and thermodynamic calculations of chemical reactions for sodium roasting of vanadium-chromium slag,the simultaneous extraction of vanadium and chromium by high sodium and low temperature roasting was proposed.The effects of particle size of vanadium chromium slag,ad...
Experimental Study on Direct Reduction of Vanadium and Titanium-bearing Sea Sand Ore Pellets in Gas-based Shaft Furnace
Yan Fangxing, Zhang Qifu, Cao Chaozhen, Hou Jian, Li Naiyao, Lan Jiran
2020, 41(4): 7-11. doi: 10.7513/j.issn.1004-7638.2020.04.002
Abstract(90) PDF(4)
Abstract:
To explore the feasibility of direct reduction of vanadium and titanium bearing sea sand ore in gas-based shaft furnace,the oxidized pellets of the ore were obtained by roasting at 1 250 ℃ for 20 min,with compressive strength of 2 099 N,reduction index(RI) of 77.8%,reduction dusting index(RDI) at lo...
Influencing Factors and Countermeasures for Vanadium Yield during Ferrovanadium Smelting in Cylinder Furnace
You Benyin
2020, 41(4): 12-17. doi: 10.7513/j.issn.1004-7638.2020.04.003
Abstract(98) PDF(1)
Abstract:
According to the characteristics of ferrovanadium smelting in cylinder furnace and the current state of vanadium recovery for ferrovanadium smelting in the world,the factors influencing the vanadium recovery were systematically analyzed,and the bulk density of vanadium oxides as well as the ramming ...
Preparation of Nano-TiO2 Thin Film by Agar Coating Method and Its Photocatalytic Degradation Performances
Dong Hongxing, Liu Qiuping, Liu Yongfeng
2020, 41(4): 18-23. doi: 10.7513/j.issn.1004-7638.2020.04.004
Abstract(94) PDF(1)
Abstract:
Nano-TiO2 thin films were prepared by agar coating method,and the photocatalytic properties of the prepared TiO2 thin films were studied.The thin films were characterized by XRD,BET,FESEM,FTIR,EDX and UV-Vis DRS.The results show that the crystal size of TiO2 prepared by agar coating can be reduced t...
Experimental Study on Sintering of Fine Ilmenite Concentrate
Wang Yujian
2020, 41(4): 24-29. doi: 10.7513/j.issn.1004-7638.2020.04.005
Abstract(174) PDF(5)
Abstract:
In view of the problems of fine particle size and high loss during electric furnace smelting of ilmenite concentrate,the sintering process of fine ilmenite concentrate was studied in this paper.It has the disadvantages of poor granulating,high burnup and low production efficiency for sintering of fi...
Gas-based Reduction Kinetics of Sintered Ilmenite Concentrate
Song Bing, Zhu Fengxiang, Shi Mingchuan, Xiao Jun, Ling Peng, Hu Yuanjin
2020, 41(4): 30-35,40. doi: 10.7513/j.issn.1004-7638.2020.04.006
Abstract(102) PDF(3)
Abstract:
In order to deeply understand the gas-based reduction mechanisms of sintered ilmenite concentrate,the isothermal reduction of the sintered ilmenite concentrate was performed under the reduction atmosphere of 30% CO and 70% N2 at 800,900 and 1 000 ℃,respectively.And the reduction kinetics was analyze...
Application of Vanadium and Titanium
Influence of Titanium on the Wear Properties of Graphene Reinforced Copper Matrix Composites
Xian Yong, Chen Deping, Liao Tingting, Ding Yichao, Wang Jing, Liu Yao
2020, 41(4): 36-40. doi: 10.7513/j.issn.1004-7638.2020.04.007
Abstract(119) PDF(1)
Abstract:
Graphene reinforced copper matrix composites were fabricated by titanium alloying and hot press sintering method.The tribological test was performed on a reciprocating tribometer.Phase was identified by X-ray diffraction(XRD) and microstructure and wear surface were determined by optical microscopy,...
Effect of Tungsten on High Temperature Plasticity of High Temperature Titanium Alloy by TiH2 Powder Metallurgy
Ma Lan, Yang Shaoli, Li Junhan, Zhu Yuling
2020, 41(4): 41-47. doi: 10.7513/j.issn.1004-7638.2020.04.008
Abstract(121) PDF(1)
Abstract:
In this paper,titanium hydride(TiH2) was used as raw material to prepare high-temperature titanium alloys by powder metallurgy.The effect of tungsten content on high temperature plasticity of the prepared Ti alloy was explored at deformation temperature of 750~900 ℃,deformation amount of 50%,and str...
Preparation and Properties of Porous Ti-Al Alloy
Zhang Meili, Luo Shushu, Dai Weili, Liu Yanfeng, Li Chun, Yang Chaopu
2020, 41(4): 48-53,59. doi: 10.7513/j.issn.1004-7638.2020.04.009
Abstract(192) PDF(3)
Abstract:
The porous Ti-Al alloys were prepared by powder metallurgy technique with elemental powder mixing,partial diffusion and reaction sintering.The effects of Al powder addition on phase structure,pore morphology,porosity,compressive properties and corrosion resistance of the alloy were investigated.The ...
Study on Microstructure and Properties of Titanium Alloy for Building by Electromagnetic Pulse Forming
Cui Mengjun, Guo Qing
2020, 41(4): 54-59. doi: 10.7513/j.issn.1004-7638.2020.04.010
Abstract(64) PDF(1)
Abstract:
The electromagnetic pulse forming test of Ti-6Al-4V-0.5Cr,a new titanium alloy for building,was carried out at different processing parameters,and the microstructure and mechanical properties of the alloy were tested and analyzed.The results show that the experimental alloys with better properties c...
Effect of WC on Microstructure and Mechanical Properties of TiC-based Cermets
Sun Qingzhu, Chen Min, Zhang Xuefeng, Wang Haibo
2020, 41(4): 60-64. doi: 10.7513/j.issn.1004-7638.2020.04.011
Abstract(89) PDF(1)
Abstract:
The effect of WC addition amount on the microstructure and mechanical properties of the TiC-based cermet was investigated using BSE,EDS and XRD.The results show that the hard phase of the cermet with WC added is constituted of white core-grey rim phase and black core-grey rim phase,both of which are...
Preparation and Properties of Vanadium-based Hydrogen Storage Alloy Based on Mechanical Vibration
Sun Chengning, Huang Wei, Zhang Junchao
2020, 41(4): 65-69. doi: 10.7513/j.issn.1004-7638.2020.04.012
Abstract(60) PDF(2)
Abstract:
The mechanical vibration with various vibration frequencies and vibration time were introduced into the pouring process to prepare V3TiNi0.56 vanadium-based hydrogen storage alloy for automobile battery,and the corrosion resistance,charge-discharge cycle stability and microstructure of the obtained ...
Technical Review
Research Progress on Precipitation Behavior of Nanoparticles in Ti-Mo Bearing Ferritic Steel
Huang Yao
2020, 41(4): 70-75. doi: 10.7513/j.issn.1004-7638.2020.04.013
Abstract(91) PDF(3)
Abstract:
The research trends of steel composition,process and mechanical properties of nano phase ferrite were introduced.The influence of composition,finishing rolling temperature,cooling rate,coiling temperature and isothermal time of different Ti systems,Ti-Mo systems and Ti-Nb systems on the behaviors an...
Research Progress of Electron Beam Vapor Deposition
Lai Qi, Li Junhan, Wu Enhui, Cui Yan, Li Liang, Liao Xianjie
2020, 41(4): 76-81. doi: 10.7513/j.issn.1004-7638.2020.04.014
Abstract(387) PDF(12)
Abstract:
This paper introduces the control of deposition,composition and structure of materials in the process of high-speed electron beam evaporation under the control of vacuum and technological parameters.The hardware conditions are briefly discussed in order to provide an understanding way for the prepar...
Resources Environment and Energy Saving
Study on Granulation Performance of Blast Furnace Slag by Gas Quenching
Wang Lili, Zhang Yuzhu, Ke Haibin, Long Yue
2020, 41(4): 82-86. doi: 10.7513/j.issn.1004-7638.2020.04.015
Abstract(127) PDF(5)
Abstract:
Gas quenching dry slag granulation process is one of the dry slag treatment processes,and granulation performance mainly includes the average diameter,size distributions and bead forming rate.The effects of different gas velocity and slag viscosity on the granulation properties were experimentally s...
Experimental Study of Fe Removal from TiC-containing Slag
Wang Dongsheng
2020, 41(4): 87-91. doi: 10.7513/j.issn.1004-7638.2020.04.016
Abstract(66) PDF(1)
Abstract:
The TiC-containing slag,which is produced by carbon reduction of BF slag,containes Fe 1.7% ~ 3.2%.In this paper,the removal of Fe from TiC-containing slag was studied by means of SEM analysis and experimental study.The results of SEM analysis indicated that the particle size of Fe in the TiC-contain...
Study on the S Content of Titanium Slag Acid Hydrolysis Tail Gas
Wang Haibo, Luo Zhiqiang, Wu Xiaoping, Ma Weiping, Wang Bin, Xing Huijin
2020, 41(4): 92-96. doi: 10.7513/j.issn.1004-7638.2020.04.017
Abstract(66) PDF(5)
Abstract:
To solve the problem of the exceeding S content in tail gas from a titanium dioxide plant,the S content of titanium ore and titanium slag raw materials was compared and analyzed.The S content of the tail gas under different acid hydrolysis conditions was simulated using sulfuric acid.Verification te...
Activation of Vanadium-titanium Magnetite Tailing and Its Application as Cement Admixture
Liu Haijun, Zhao Lili
2020, 41(4): 97-102. doi: 10.7513/j.issn.1004-7638.2020.04.018
Abstract(80) PDF(1)
Abstract:
In this study,mechanical activation and chemical activation methods were used to improve the activity of cement mortar.The effects of activation methods on the structure and properties of tailings were studied.The influences of activation conditions and tailings amount on the mechanical strength of ...
Ferrous Metallurgy and Materials
Effect of Dephosphorization Agent on Gasification and Dephosphorization of High Phosphorus Iron Ore Pellets
Guo Yuanzheng, Li Jie, Li Fei, Li Daliang, Liu Wenqiang, Cheng Yang
2020, 41(4): 103-107,114. doi: 10.7513/j.issn.1004-7638.2020.04.019
Abstract(130) PDF(2)
Abstract:
The development and utilization of high-phosphorus iron ore are restricted due to its high content of phosphorus.The occurrence state of phosphorus in high-phosphorous iron ores had been investigated by XRD diffraction.And based on the thermodynamic calculation results of FactSage7.2,the measures of...
Numerical Simulation of Electromagnetic Stirring in Billet Mold
Li Yaoguang, Wang Hongbin, Bai Xuesong, Sun Yanhui, Zhang Minghai, Jia Jianping
2020, 41(4): 108-114. doi: 10.7513/j.issn.1004-7638.2020.04.020
Abstract(129) PDF(3)
Abstract:
In this study a three-dimensional mathematical model of electromagnetic stirring in billet mold was developed by adopting ANSYS finite element analysis software.The effects of different process parameters on magnetic flux density and electromagnetic force in the billet mold were discussed.It is foun...
Thermodynamic Study on the Precipitation Behavior of Carbonide and Nitride in X80 Pipeline Steel
Feng Qian, Ceng Yanan, Li Junguo, Tang Guozhang
2020, 41(4): 115-120. doi: 10.7513/j.issn.1004-7638.2020.04.021
Abstract(98) PDF(3)
Abstract:
In order to clarify the precipitation rule of precipitated particles in the solidification process of X80 pipeline steel,the Thermo-calc software was used to analyze the austenite and ferrite phase transition temperature,the type of precipitates,the precipitation temperature of the precipitates and ...
Effect of Mn on Microstructure and Mechanical Properties of ULC Ti Microalloyed SM490A
Qin Xiangzhi, Lü Yuan, Xie Guoqing, Qi Haiquan
2020, 41(4): 121-124. doi: 10.7513/j.issn.1004-7638.2020.04.022
Abstract(155) PDF(1)
Abstract:
In the process of developing ULC SM490 A by Ti microalloying,excessive strength fluctuation was caused by different Mn content. Therefore,the influence of Mn on the microstructure and mechanical properties of ULC Ti microalloy steel has been studied. It is found out that when the Mn content was incr...
Research on Redissolution Behavior of Nb and Ti in the High Strength Pipeline Steel
Ren Yi, Gao Hong, Liu Wenyue, Zhang Shuai, Wang Shuang
2020, 41(4): 125-129. doi: 10.7513/j.issn.1004-7638.2020.04.023
Abstract(69) PDF(1)
Abstract:
In this study,the redissolution and precipitation behaviors of niobium titanium carbonitride(Nb,Ti)(C,N) were researched by electrolytic phase analysis method and calculated by the simplified thermodynamic calculation method,and the dissolution law of Nb and Ti elements in high Nb pipeline steel was...
Research on Carbide Control of High Speed Steel
Liang Wei, Li Jing, Shi Chengbin, Zhang Jie
2020, 41(4): 130-138. doi: 10.7513/j.issn.1004-7638.2020.04.024
Abstract(246) PDF(3)
Abstract:
The types,production process and development status of high speed steel are summarized.The effects of ESR process,hot processing deformation process,heat treatment process,cryogenic treatment and modification treatment on the carbides in high speed steel production,which are mainly based on smelting...
Effects of Heat-treatment Processes on Microstructures and Properties of a 1 000 MPa Grade Vanadium-alloyed High Strength Steel
Zhang Gongting, Tang Di, Zheng Zhiwang, Zhao Zhengzhi
2020, 41(4): 139-144. doi: 10.7513/j.issn.1004-7638.2020.04.025
Abstract(188) PDF(4)
Abstract:
The 0.24%C-1.5%Si-2.0%Mn-0.16%V cold-rolled steel was heat treated at 780 ℃ intercritical annealing for 180 s,then quenching into 350~380 ℃ for 360 s,or quenching into 380 ℃ for holding 60~1 200 s.The microstructures and properties after heat treatments were tested by tension test,OM,SEM and XRD ana...
Effect of Annealing Process on Microstructure and Mechanical Properties of 1 180 MPa Dual Phase Steel
Zhen Weijing, Chen Jundong, Li Yongliang, Wang Fuming
2020, 41(4): 145-149. doi: 10.7513/j.issn.1004-7638.2020.04.026
Abstract(96) PDF(1)
Abstract:
The influence of annealing process on microstructure and mechanical properties of super high strength steel DP1180 was studied by means of thermo-simulator system Gleeble-3500,field emission scanning electron microscopy and transmission electron microscope.The results show that the yield strength de...
Effects of Pre-strain and Baking Temperature on the Microstructure and Bake-hardening Behavior of Mild Steel and Dual Phase Steel
Kuang Chunfu
2020, 41(4): 150-156. doi: 10.7513/j.issn.1004-7638.2020.04.027
Abstract(276) PDF(2)
Abstract:
In a typical process,mild steel and dual phase steel were respectively annealed at 800 ℃ for 90 s,cooled slowly to 680 ℃ and then cooled rapidly to 300 ℃ to carry out the overaging treatment.As a result,the ferrite-cementite mild steel and ferrite-martensite dual phase steel were obtained after the ...
Study of Low Tempering Temperature on Microstructure and Properties of Cold-drawn Pearlite Steel Wires
Hu Yanan
2020, 41(4): 157-161. doi: 10.7513/j.issn.1004-7638.2020.04.028
Abstract(178) PDF(5)
Abstract:
The properties and structure changes of a cold-drawn pearlite steel wire annealed at 200~300 ℃ were studied,and the strengthening and toughening mechanism during tempering was revealed by means of scanning electron microscopy,transmission electron microscopy,X-ray diffraction and conventional mechan...
Study on Influencing Factors of Corrosion Resistance of Hot Dip Galvanized Fingerprint Sheet
Hu Huadong, Kang Yefeng, Cha Kai, Dong Lihua
2020, 41(4): 162-167. doi: 10.7513/j.issn.1004-7638.2020.04.029
Abstract(115) PDF(3)
Abstract:
In this study a lot of production verification and test had been conducted to find the factors that influence the corrosion performance of fingerprint resistant sheet. It is found out that the corrosion resistant properties of hot dip galvanized fingerprint resistant mainly relates to drying tempera...
Optimization of Smelting Performance of Oxy-combustion Melting Furnace
Kong Zheng, Zhao Kai, Shi Xuefeng, Zhang Qiaorong, Shi Yan, Zhang Xiaohua
2020, 41(4): 168-176. doi: 10.7513/j.issn.1004-7638.2020.04.030
Abstract(95) PDF(2)
Abstract:
In this paper,the oxy-combustion melting furnace developed by a company had been taken as the research object.Based on the VOF multi-phase flow model and the Realizable k-ε model,the gas-liquid two-phase flow in the molten pool area of the melting furnace had been numerically simulated.Under the sta...