2019 Vol. 40, No. 5

Separating and Extracting of Vanadium and Titanium
Preparation and Consolidation Technology of Vanadium Slag Pellets
Guo Jike, Fu Zibi, Ye Lu, Jiang Lin
2019, 40(5): 1-7. doi: 10.7513/j.issn.1004-7638.2019.05.001
Abstract(81) PDF(2)
Abstract:
In order to solve the production problem of poor performances of vanadium slag pellets during the process of sodium salt roasting and hot water leaching of vanadium slag pellets,the technology of pelletizing and drying for vanadium slag fine powder was studied.The laboratorial and industrial test re...
Desilication from Alkali Leaching Solution Containing Vanadium and Preparation of High Purity Vanadium Pentoxide
Liu Bo
2019, 40(5): 8-15,36. doi: 10.7513/j.issn.1004-7638.2019.05.002
Abstract(161) PDF(14)
Abstract:
Using the alkaline leaching solution containing vanadium produced by a factory in Panzhihua as the raw material,the main impurities and the removal of silicon in the alkaline leaching solution were analyzed,and the influences of desilication agent species,dosage of desilication agent,pH of leaching ...
Effects of Vanadium Concentration and Sulfuric Acid Concentration on the Electrochemical Properties of Negative Electrolyte for Vanadium Redox Flow Battery
Han Huiguo
2019, 40(5): 16-22,43. doi: 10.7513/j.issn.1004-7638.2019.05.003
Abstract(264) PDF(8)
Abstract:
In order to improve the electrochemical activity and energy density of negative electrolyte of vanadium redox flow battery,the viscosity,conductivity and electrochemical performances of the negative electrolytes at different compositions were investigated.The results show that the vanadium concentra...
Preparation and Study of Heavy Metal Ion Doped TiO2 Photocatalyst Powder
Zhou Shijie, Qiu Kehui, Gong Yanli, Li Junfeng, Zhang Peicong, Zhang Wentao, Long Jianping
2019, 40(5): 23-26. doi: 10.7513/j.issn.1004-7638.2019.05.004
Abstract(103) PDF(2)
Abstract:
TiO2 powder was prepared by sol-gel method using butyl titanate(C16H36O4Ti4) as the titanium source and anhydrous ethanol(C2H6O) as the organic solvent respectively,and then the obtained TiO2 was doped with copper and silver.The products were characterized by scanning electron microscopy(SEM) and X-...
Effects of Carbon Content and Nitrogen Pressure on Synthesis of Ti2Al(C, N)
Xian Yong, Luo Chuandong, Chen Deping, Ding Yichao, Wang Jing
2019, 40(5): 27-30. doi: 10.7513/j.issn.1004-7638.2019.05.005
Abstract(57) PDF(1)
Abstract:
Ti2Al(C,N)was synthesized by hot pressing sintering under different carbon content and nitrogen pressure.The phase was analyzed by X-ray diffraction(XRD).The three-point bending strength was tested and the fracture morphology was analyzed by scanning electron microscopy(SEM).The results showed that ...
Preliminary Study of Preparing Macroporous Titanium Dioxide Material from Panzhihua Ilmenite
Zhang Jianbo
2019, 40(5): 31-36. doi: 10.7513/j.issn.1004-7638.2019.05.006
Abstract(59) PDF(2)
Abstract:
Macroporous TiO2,with the pore size higher than 50 nm,is an important material.This paper proposed and preliminarily studied a method for preparing macroporous titanium dioxide(rutile) from Panzhihua ilmenite by two steps of thermal pretreatment-hydrochloric acid leaching.The results show that both ...
Application of Vanadium and Titanium
Welding and Heat Treatment Procedures Research of New Titanium Alloy Ti-3Al-2Mo-2Zr(TA24)
Du Yongqin, Zhu Jinfei, Zhang Jianxiang, Wang Niwen
2019, 40(5): 37-43. doi: 10.7513/j.issn.1004-7638.2019.05.007
Abstract(184) PDF(7)
Abstract:
Based on the chemical compositions,microstructure and mechanical properties of new titanium-alloy Ti-3Al-2Mo-2Zr(TA24),the properties at typical high temperatures of the alloy were investigated.The test plates of the alloy were welded by GTAW,and the postweld heat treatment was carried out at specif...
Effect of VC on Microstructure and Mechanical Properties of TiC-based Cermets
Chen Min, Zhang Xuefeng
2019, 40(5): 44-49. doi: 10.7513/j.issn.1004-7638.2019.05.008
Abstract(96) PDF(1)
Abstract:
The effect of VC addition amount on the microstructure and mechanical properties of the TiC-based cermet at different temperatures was investigated using BSE,EDS,XRD and density,hardness,bending strength tests.The results show that the core and rim phases in the TiC-based cermet have the same crysta...
Effect of Titanium Hydride Content on Near-alpha Multicomponent High Temperature Titanium Alloy
Zhu Yuling, Yang Shaoli, Ma Lan, Piao Rongxun
2019, 40(5): 50-54. doi: 10.7513/j.issn.1004-7638.2019.05.009
Abstract(207) PDF(3)
Abstract:
Near-alpha multicomponent high temperature titanium alloy was prepared through powder metallurgy using titanium hydride and titanium powder as the main raw materials,and the effect of titanium hydride content on the microstructure and mechanical properties of the alloy was investigated.The results s...
Study on Thermal Insulation Properties of Nano-VO2 Modified Plexi Glass
Tang Lu, Huang Wanxia, Wen Hao, Zhou Li
2019, 40(5): 55-60. doi: 10.7513/j.issn.1004-7638.2019.05.010
Abstract(150) PDF(4)
Abstract:
In this paper,the plexi glass with infrared intelligent heat insulation was prepared respectively at low and high temperature polymerization conditions,via adding nano-vanadium dioxide slurry obtained from nano-vanadium dioxide powder into the prepolymerof methyl methacrylate.The plexi glass with in...
Microstructure and Properties of New Automobile Magnesium Alloy Modified by Vanadium and Titanium
Zhuang Yanxia, Li Ning
2019, 40(5): 61-65. doi: 10.7513/j.issn.1004-7638.2019.05.011
Abstract(62) PDF(1)
Abstract:
In order to optimize the quality and properties of Mg-8Al-0.6Zn alloy for automobile,vanadium-titanium modification of Mg-8Al-0.6Zn-xV-0.5Ti(x=0,0.1,0.5,0.8) specimens was carried out,and the microstructure and mechanical properties of specimens with different vanadium content were tested and analyz...
Extrusion Process Optimization of Vanadium-bearing Aluminium Alloy for Mechanical Shell
Wang Jinghui, Shang Lifeng, Zhao Liqiang
2019, 40(5): 66-70. doi: 10.7513/j.issn.1004-7638.2019.05.012
Abstract(55) PDF(1)
Abstract:
In this paper,new vanadium-bearing aluminum alloy 6061-0.8 V specimens for mechanical shell were extruded at different extrusion speeds and temperatures,and the mechanical properties were tested and analyzed.The results show that when extrusion speed is increased from 2 m/min to 4.5 m/min and the ex...
Resources Environment and Energy Saving
Effect of Gas Quenching Behavior of Modified Steel Slag on Digestion of f-CaO
Guo Chen, Zhang Wei, Wang Hui, Xing Hongwei
2019, 40(5): 71-77. doi: 10.7513/j.issn.1004-7638.2019.05.013
Abstract(86) PDF(2)
Abstract:
In this paper blast furnace slag with different content(0%,15%,25%,35%) was selected to carry out quenching and tempering reconstruction on steel slag,and then high-temperature gas quenching had been performed.Influence of gas quenching behavior on the elimination of f-CaO by reconstructed slag had ...
Effect of Fe(OH)3 on the Mechanical Properties of Titanium Gypsum by Gypsum Enhancer
Yang He, Chen Wei
2019, 40(5): 78-83. doi: 10.7513/j.issn.1004-7638.2019.05.014
Abstract(70) PDF(1)
Abstract:
In this paper the effect of Fe(OH)3 on the improvement of mechanical properties of titanium gypsum through addition gypsum enhancer had been investigated.The experimental results indicate that the effect of gypsum enhancer on improving the mechanical properties of titanium gypsum is significantly re...
Microwave Combined Modified Activated Carbon for Treatment of Flue Gas Desulfurization Efficiency of Different Concentrations of SO2
Shi Yan, Kong Zheng, Hu Changqing, Zhao Ying, Wang Shuai, Zhao Xin
2019, 40(5): 84-88. doi: 10.7513/j.issn.1004-7638.2019.05.015
Abstract(80) PDF(1)
Abstract:
Activated carbon was used as the research object,and the simulated flue gas with different concentrations of SO2 was processed by microwave irradiation.Through varying microwave heating temperature,heating time,activated carbon quality,flue gas flow rate and SO2 concentration,the factors influencing...
Effect of MgO/Al2O3 on Crystallization Behavior of Molten Modified Slag in Preparation Process of Blast Furnace Slag Based Cotton
Yao Jianxin, Bian Miaolian, Du Peipei
2019, 40(5): 89-94,103. doi: 10.7513/j.issn.1004-7638.2019.05.016
Abstract(62) PDF(2)
Abstract:
In order to explore the effect of MgO/Al2O3 ratio on crystallization behavior of molten modified slag in the preparation progress of blast-furnace-slag-based slag fiber,theoretical crystallization temperature and species and contents of precipitated phases at different values of MgO/Al2O3 ratio in c...
Ferrous Metallurgy and Materials
Research on the Carbothermic Reduction Kinetic of Oolitic Hematite with Graphite at 1 173~1 473 K
Chen Wen, Lei Ying, He Siqi, Liao Zhenhong, Wang Xuesong
2019, 40(5): 95-103. doi: 10.7513/j.issn.1004-7638.2019.05.017
Abstract(66) PDF(1)
Abstract:
The carbothermic reduction kinetics of oolitic hematite with graphite was investigated at temperature of 1 173~1 373 K by using thermogravimetric method.The effects of temperature on reduction degree and reaction rate were studied.The reduction reactions were fitted to several solid-state reaction m...
Study on Indirect Reduction Law in Carbothermal Reduction Process for Iron Oxide
Guo Peimin, Zhao Pei, Kong Lingbing, Wang Lei
2019, 40(5): 104-109. doi: 10.7513/j.issn.1004-7638.2019.05.018
Abstract(352) PDF(9)
Abstract:
In order to study the law of indirect reduction in the process of carbothermal reduction,experiments were carried out on a 20 kg/h pushing boat heating furnace.The changes of gas composition in the process were recorded by on-line gas analyzer,and composition of reduced samples was measured.The infl...
Study on Melting Carburization Behavior of Flash Ironmaking
Zhang Liangliang, Dai Xi
2019, 40(5): 110-119. doi: 10.7513/j.issn.1004-7638.2019.05.019
Abstract(234) PDF(10)
Abstract:
The final carbon content of the molten iron is saturated during the traditional blast furnace smelting process.However,the reaction in the flash furnace occurs at the stage of material floating and the carburizing effect of the solid charge and the molten iron in the blast furnace cannot occur witho...
Study on Mineralogical Structures and Metallurgical Properties of Acid Pellets
Ding Shangshang, Liu Lei, Han Xiuli, Zhang Di, Zhou Xiang
2019, 40(5): 120-125. doi: 10.7513/j.issn.1004-7638.2019.05.020
Abstract(171) PDF(2)
Abstract:
The mineral composition and microstructures of pellets are important factors affecting their metallurgical properties.The mineral types,contents,morphology,size,distribution and pore characteristics of acid pellets from different steel works were quantitatively studied by polarizing microscope and X...
Effect of MgO/Al2O3 and Burden Structure on Droplet Properties of Comprehensive Burden
Ma Baoliang, Zhang Yuzhu, Pan Xiangyang, Long Yue, Li Shenzi, Du Peipei
2019, 40(5): 126-132. doi: 10.7513/j.issn.1004-7638.2019.05.021
Abstract(90) PDF(3)
Abstract:
Effect of MgO/Al2O3 and burden structure on droplet properties of comprehensive burden was studied by simulating actual blast furnace smelting conditions in high temperature drop furnace.The results show that when MgO/Al2O3 increases from 0.9 to 1.0,the softening and melting temperatures of furnace ...
Effect of Copper Nitrate on the Preparation of α-Fe2O3 Powder and its Photo-catalytic Performance
Cao Zhiqin, Zuo Chengyang, Liu Wei, Zhang Xuefeng
2019, 40(5): 133-137. doi: 10.7513/j.issn.1004-7638.2019.05.022
Abstract(80) PDF(3)
Abstract:
The α-Fe2O3 nano-composites with photo-catalytic activity were prepared by solution combustion synthesis using ferric nitrate,copper nitrate and glycine as raw materials.The grain size of α-Fe2O3 is about 30 nm.The products were characterized by XRD,SEM and TEM.The effects of copper nitrate content ...
Study on Dephosphorization of Coke Reduction Converter Slag by Gasification
Wang Shuhuan, Guo Ruihua, Zhou Chaogang, Zhao Dingguo, Xue Yuekai, Li Chenxiao, Liu Shiqi
2019, 40(5): 138-142. doi: 10.7513/j.issn.1004-7638.2019.05.023
Abstract(68) PDF(2)
Abstract:
In order to solve the problem that phosphorus content in slag is too high to be recycled directly in converter,the influence of different temperature,alkalinity,FeO content and nitrogen flow rate on gasification dephosphorization rate was systematically studied by means of related hot state experime...
Development and Application of Capping Delayed Running Out Process for Large Round Bloom Continuous Casting
Chen Yuanqing, Qiu Shengtao, Liu Heping, Li Shangbing, Qiu Hao
2019, 40(5): 143-149. doi: 10.7513/j.issn.1004-7638.2019.05.024
Abstract(90) PDF(3)
Abstract:
The difference of solidification structure and macro quality between trail bloom and normal bloom has been comparatively analyzed for ø380~ø800 mm large round bloom. Some defects such as low ratio of equiaxed crystal zone,high ratio of white band,serious central porosity,cavity and crack are observe...
Effect of Solution Treatment on the Austenite Grain Growth of GH3128 Alloy
Jiang Shichuan, Zhang Jian, Liu Tingyao, Lai Yu
2019, 40(5): 150-156. doi: 10.7513/j.issn.1004-7638.2019.05.025
Abstract(173) PDF(4)
Abstract:
In this paper,the effect of solution temperature and holding time on austenite grain growth of GH3128 alloy was studied.The results show that,with the increase of solution temperature and holding time,the austenite grain size of the alloy increases gradually.Compared with the effect of holding time,...
Influence of Filler Metal and Current on Microstructure and Properties of 0Cr18Ni9/Q235 Dissimilar Welded Joints
Chen Jinliang, Pan Deng
2019, 40(5): 157-161. doi: 10.7513/j.issn.1004-7638.2019.05.026
Abstract(178) PDF(4)
Abstract:
The Tungsten Inert Gas(TIG) welding process was used to weld 0Cr18Ni9 austenitic stainless steel and Q235 carbon steel with ER309 and Ni317 wires of 2.0 mm in diameter.The microstructure,tensile properties and micro-hardness of the welded joint were studied.The results show that when the applied wel...
Effect of Heat Treatment Process on Liquid-precipitated Carbides in MC5D roller Blank for Cold-rolling Application
Lin Faju
2019, 40(5): 162-168. doi: 10.7513/j.issn.1004-7638.2019.05.027
Abstract(111) PDF(5)
Abstract:
In this paper,the effect of heat treatment process on liquid-precipitated carbides in MC5D cold-rolling roller blank was investigated.The phase transformation and type of carbides in MC5D steel at equilibrium state were calculated by JMatoPro software,and the microstructure of the blank was observed...
Study on Low Temperature Characteristics of UHV Q460 Steel Tube Tower
Huang Yao, Zhu Binrong, Bai Zhang, Su Zhigang, Liu Weining, Jiang Zhanbin
2019, 40(5): 169-175. doi: 10.7513/j.issn.1004-7638.2019.05.028
Abstract(100) PDF(4)
Abstract:
The mechanical properties,impact toughness and fracture morphology of Q460 steel pipes of different specifications and different quality grades at different test temperatures were studied by means of scanning electron microscopy,mechanical properties test and Charpy impact test.The influences of wal...
Analysis of Pockmarks Formed on the Surface of 20Cr13 Martensitic Stainless Steel
Zhou Peng, Cui Shan
2019, 40(5): 176-180. doi: 10.7513/j.issn.1004-7638.2019.05.029
Abstract(159) PDF(3)
Abstract:
The surface defects of martensitic stainless-steel table knives were analyzed.The macro-morphology and characteristic of pockmark defects on the surface of martensitic stainless steel were described,and the micro-morphology and component were analyzed by scanning electronic microscopy and energy dis...