2016 Vol. 37, No. 1

Separating and Extracting of Vanadium and Titanium
Experimental Study on the Flotation of Ilmenite in the Onkilonite of Vanadium-titanium Magnetite Using MOH as the Collector
Liu Weijun, Wang Weiqing, Yan Wu, Deng Jie, Zhang Shiqiu, Ren Pengkun
2016, 37(1): 1-6. doi: 10.7513/j.issn.1004-7638.2016.01.001
Abstract(83) PDF(2)
Abstract:
The flotation of ilmenite in the onkilonite of vanadium-titanium magnetite using MOH as the collector was investigated.The effects of dosage of MOH,H2SO4 and sodium silicate on separation of ilmenite and gangue minerals were studied.The open and closed circuit experiments for ilmenite flotation were...
Effect of Pre-oxidation on Pulverization of Yunnan Titanium Concentrate during Hydrochloric Acid Leaching
Lin Fan, Yang Jian, Chen Kui, Zhao Dong, Liu Songli, Liu Guoqing
2016, 37(1): 7-11. doi: 10.7513/j.issn.1004-7638.2016.01.002
Abstract(73) PDF(3)
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Synthetic rutile as a good substitute for natural rutile is greatly used for production of titanium dioxide by chlorination process and sponge titanium.According to the physical and chemical properties of Yunnan titanium concentrate,pre-oxidation and hydrochloric acid leaching method was used to pre...
Technology Research on Sodium Salt Roasting of Vanadium Slag Pellet
Yin Zhaoqian, Li Qianwen, Fu Zibi, Wang Jun, Gao Guanjin
2016, 37(1): 12-15,20. doi: 10.7513/j.issn.1004-7638.2016.01.003
Abstract(95) PDF(1)
Abstract:
Roasting of vanadium slag pellets containing sodium carbonate were investigated in this paper.This technology can avoid sintering of raw materials during roasting without addition of residual slag of vanadium extraction,and substantially increases calcination efficiency of vanadium slag coupled with...
Technology Research on Dispersity of Titanium Dioxide
Chen Xinhong, Zheng Shaohua, Li Chun
2016, 37(1): 16-20. doi: 10.7513/j.issn.1004-7638.2016.01.004
Abstract(240) PDF(10)
Abstract:
The "dispersing and grinding"combined process was studied for dispersing TiO2.The dispersity of TiO2 particles was characterized as viscosity and particle size.The particle size and morphology of TiO2 before and after dispersing were observed using TEM.Effects of the dispersing agents and their addi...
Removal of Arsenic from Vanadium-chromium Containing Solution by Ferric Salt
Luo Xiang, Wu Zhenxiu, Fu Zibi, Su Yi
2016, 37(1): 21-25. doi: 10.7513/j.issn.1004-7638.2016.01.005
Abstract(59) PDF(0)
Abstract:
According to the higher arsenic content in the leaching solution of roasted vanadium slag produced in steel making with vanadium titanium magnetite from Hongge south mining area,ferric salt was used for arsenic removal to prepare high purity V2O5.The effects of initial pH,reaction temperature and ti...
Study on Sulfuric Acid Leaching of Vanadium-containing Clinker by Calcified Roasting
Wang Chunqiong
2016, 37(1): 26-30,36. doi: 10.7513/j.issn.1004-7638.2016.01.006
Abstract(96) PDF(4)
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According to the lower leaching rate of vanadium-containing clinker by calcified roasting in industrial production,effects of the clinker particle size,magnetic materials content and temperature on the leaching rate of vanadium were investigated.The results show that the decrease in leaching rate is...
Application of Vanadium and Titanium
Controlling on Front End Bending during Hot Finish Rolling Process of Pure Titanium Coil
Li Jun, Yu Hui, Shi Qingnan, Peng Lin
2016, 37(1): 31-36. doi: 10.7513/j.issn.1004-7638.2016.01.007
Abstract(67) PDF(1)
Abstract:
Front end bending is a common phenomenon in the hot rolling process of plate and strip.Aiming at this problem,in this work,the finite element method was used to study the metal flow of the rolling deformation zone for hot rolling pure titanium coil.The results show that the metal flow of pure titani...
Effect of Second Annealing on Properties and Microstructures of Commercial Pure Titanium
Jiang Qingwei, Yang Jie
2016, 37(1): 37-40. doi: 10.7513/j.issn.1004-7638.2016.01.008
Abstract(192) PDF(10)
Abstract:
The microstructures and mechanical properties of cold rolled commercial pure titanium after second annealing was studied.The results show that:the second annealing has no effect on grain size of the factory state pure titanium belt,but it plays an important role in improving the commercial pure tita...
Microstructure and Properties of the New-typed TiNi-based Shape Memory Alloy for Micro Electro Mechanical System
Shi Zengfang
2016, 37(1): 41-45. doi: 10.7513/j.issn.1004-7638.2016.01.009
Abstract(73) PDF(0)
Abstract:
The new-typed TiNi-based shape memory alloy TiNi45V8In0.2 for micro electro mechanical system was successfully prepared by the method of two-step.The alloy was analyzed by XRD,SEM and so on.And the mechanical properties,stress relaxation resistance and corrosion resistance were tested and analyzed.T...
Preparation of Fe-Ti(C,N) Composites from Titanomagnetite Concentrate by Carbothermal Reduction in Air Atmosphere
Wu Enhui, Zhu Rong, Yang Shaoli, Li Hong, Li Jun, Hou Jing
2016, 37(1): 46-50. doi: 10.7513/j.issn.1004-7638.2016.01.010
Abstract(66) PDF(1)
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Fe-TiC1-xNxcomposites were successfully prepared directly from titanomagnetite concentrate by carbothermal reduction in air atmosphere.The influences of reduction temperature and carbon content on the reaction process and phase evolution during carbothermal reduction of titanomagnetite concentrate w...
Studying the Electrochemical Deposition of Manganese on the Surface of TiO2 Nanotube Array by Orthogonal Test
Xiong Zhongping, Si Yujun, Li Minjiao, Feng Juping
2016, 37(1): 51-55. doi: 10.7513/j.issn.1004-7638.2016.01.011
Abstract(53) PDF(1)
Abstract:
TiO2 nanotube array(TNA) was prepared by electrochemically anodizing titanium sheet.Metal manganese was deposited on the surface of TNA by electrochemical reduction to enhance its photoelectrochemical response to visible light.The influences of deposition voltage,time and concentration of Mn(II) ion...
Research on Absorption Properties of Ti-doped Short Carbon Fiber/epoxy Resin Composites by Terahertz Time Domain Spectroscopy
Deng Chaoyue, Hu Chengyao, Huo Jichuan
2016, 37(1): 56-60. doi: 10.7513/j.issn.1004-7638.2016.01.012
Abstract(107) PDF(0)
Abstract:
Terahertz is the last researched band of the electromagnetic waves,which occupies an important position in the field of stealth and anti-stealth research in the future.TiO2,Fe-TiO2 and Ba TiO3 nanoparticles were prepared by sol-gel method,and then they were doped into short carbon fiber/epoxy resin ...
Vanadium-titanium Composite Infiltration Process on the Surface of Cold Working Die Steel
Liu Weidong, Lin Cuiqing
2016, 37(1): 61-64. doi: 10.7513/j.issn.1004-7638.2016.01.013
Abstract(61) PDF(0)
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Vanadium-titanium composite infiltration coating was produced on the surface of Cr12MoV cold working die steel for different time respectively with V2O5 and TiO2 as vanadium and titanium donor,and the microstructure,phase structure,corrosion and wear resistance were tested and analyzed.The results s...
Computer Simulation for Thermo- mechanical Coupling of Friction Stir Welding of Titanium Alloy with High Melting Point
Hu Yu, Kong Jian
2016, 37(1): 65-71. doi: 10.7513/j.issn.1004-7638.2016.01.014
Abstract(90) PDF(1)
Abstract:
Based on models for heat transfer and solid mechanics of linear elastic materials with consideration of characteristics that the thermal physical properties of the titanium alloy change with temperature,the thermo-mechanical coupling model for friction stir welding(FSW) of high melting point alloy w...
Resources Environment and Energy Saving
System Design and Preparation of Glass-ceramics Using Titanium Blast Furnace Slag
Li Yaohui, Yang Zhiyuan, Wang Jinzhen, Huang Yourong
2016, 37(1): 72-78. doi: 10.7513/j.issn.1004-7638.2016.01.015
Abstract(70) PDF(1)
Abstract:
A new CaO-Al2O3-SiO2 glass-ceramics were prepared using natural cooling titanium blast furnace slag,and the effects of different systems of nucleating agents on the crystallization,microstructure and properties of the glass-ceramics were also studied by DSC,XRD,SEM,etc.The results indicate that high...
Mechanism of Recovering Iron and Zinc from BF Gas Slime by Self-reduction
Zhu Kuisong, Liu Songli, Gou Shuyun, Zhou Lanhua, Sun Yan
2016, 37(1): 79-84,89. doi: 10.7513/j.issn.1004-7638.2016.01.016
Abstract(53) PDF(0)
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The heating self-reduction process of blast furnace(BF) gas slime was studied by non-isothermal thermogravimetric(TG) analysis and isothermal heating in Muffle Furnace.The equilibrium compositions and metallization rate of iron and zinc oxides for BF gas slime in reduction process were calculated by...
Ferrous Metallurgy and Materials
Effects of Carbon Content on Sintering Performance of Vanadium Titanium Magnetite
Liu Weixing, Li Xiu, Li Jie, Tian Tielei, Long Yue
2016, 37(1): 85-89. doi: 10.7513/j.issn.1004-7638.2016.01.017
Abstract(71) PDF(1)
Abstract:
In order to understand the impact of carbon ratio on metallurgical properties and physical effects of vanadium titanium sinterthe strength,yield and particle size composition and metallurgical properties of resulting vanadium titanium sinter at various carbon ratio of 2.5%,2.75%,3.0%,3.25%,3.0%,3.75...
Effects of Low Titanium Sintering Parameters on Softening Properties of Burden Load
Li Yanjiang, Lü Qing, Bai Ruiguo, Cao Lihua, Huang Honghu, Liu Xiaojie
2016, 37(1): 90-94. doi: 10.7513/j.issn.1004-7638.2016.01.018
Abstract(89) PDF(0)
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In order to provide a more comprehensive guide to sinter production and to determine the appropriate parameters of low sintering titanium sinter in Xuanhua Steel,the impact of basicity,carbon content,MgO content,SiO2 content,moisture on burden load softening properties had been investigated by RUL t...
Research of Al2O3 Influence on Furnace Burden's Dropping Performance of Vanadium-titanium Magnetite
Wang Fujia, Lü Qing, Chen Shujun
2016, 37(1): 95-99. doi: 10.7513/j.issn.1004-7638.2016.01.019
Abstract(57) PDF(0)
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Experiments were carried out in the lab to simulate dropping zone of blast furnace by a high temperature oven,and the effect of Al2O3 on charge softening temperature range,melting temperature range,maximum pressure and other high temperature physical properties had been investigated.The results show...
Selection of Alloy Design for Low-temperature Toughness Plates Used for Line Pipes
Kathayat T S, Goyal Rajesh K, Shant Raghu, Khadia Sohanlal
2016, 37(1): 100-103. doi: 10.7513/j.issn.1004-7638.2016.01.020
Abstract(59) PDF(0)
Abstract:
The low toughness and poor weldability of the higher carbon steel grades restricted their acceptability for line pipe steel,and therefore,created good demand of low carbon micro-alloyed steels for line pipe steel for both onshore and offshore applications.In low carbon micro-alloyed steels,alloy des...
Influence of Titanium on Strength of Weldable Wire Rod ER50-G Steel
Chen Tao, Li Hong, Tong Qian, Lü Naibing, Wu Keng
2016, 37(1): 104-109. doi: 10.7513/j.issn.1004-7638.2016.01.021
Abstract(56) PDF(1)
Abstract:
The chemical compositions,mechanical properties,microstructure and precipitates of the weldable wire rod ER50-G produced by Shougang were detected and analyzed statistically in this study.The influence of titanium on the microstructure and precipitates of ER50-G and therefore the tensile strength wi...
Effect of Ti on Austenite Grain Growth Behavior in Medium Carbon Manganese Steel
He Yingying, Cao Liqiang, Ma Han
2016, 37(1): 110-115. doi: 10.7513/j.issn.1004-7638.2016.01.022
Abstract(99) PDF(0)
Abstract:
Effect of Ti on austenite grain growth behavior in medium carbon manganese steel at different heating temperature and time were studied.The results show that Ti-bearing steel exhibited a much sluggish growth rate of austenite grain compared with Ti-free counterpart at higher heating temperature,whic...
Analysis of TiN Precipitation Behavior during Solidification of Bearing Steel
Zhao Junpu, Liu Liu, Fan Jianwen, Wang Le
2016, 37(1): 116-121. doi: 10.7513/j.issn.1004-7638.2016.01.023
Abstract(55) PDF(0)
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The inclusions in bearing steel continuous casting bloom were observed,and the large size TiN inclusions were found in the bloom.The effects of Ti and N elements segregation at the solidification front on precipitation of TiN inclusion was studied on the basis of thermodynamics and dynamics.The ther...
Thermodynamic Analysis of Components Variation on the Inclusions Precipitation in GCr15 Bearing Steel during Solidification
Tang Guozhang, Ceng Yanan, Li Junguo, Fu Guoqiang, Gao Zhiyuan
2016, 37(1): 122-126. doi: 10.7513/j.issn.1004-7638.2016.01.024
Abstract(95) PDF(1)
Abstract:
The evolution of non-metallic inclusions in the GCr15 bearing steel during solidification with different content of[Ca],[Al],[O]and[Mg]was investigated by Fact Sage software which is based on minimum Gibbs free energy principle.The results showed that the inclusion types changed from CaO·2MgO·8Al2O3...
Optimization Research of Annealing Process for Silicone Modified M2 High Speed Steel
Wang Hongxia, Zhao Hui
2016, 37(1): 127-130,136. doi: 10.7513/j.issn.1004-7638.2016.01.025
Abstract(146) PDF(1)
Abstract:
Different annealing temperature and annealing time were adopted for annealing treatment of M2-1.0Si silicone modified M2 high speed steel.Through the test and analysis of the microstructure and high temperature mechanical properties,it is found that the annealing temperature and annealing time had i...
Defects Analysis and Control Measures of Continuous Casting Product
Gao Ju, Han Penglong, Gao Chunqun, Ma Yanjie, Ma Lixing
2016, 37(1): 131-136. doi: 10.7513/j.issn.1004-7638.2016.01.026
Abstract(150) PDF(7)
Abstract:
Quality defects such as edge crack,roll,strip edge uplift,oxide scale indentation usually occurred in the strip produced in a 1700 hot strip line.In order to eliminate these defects,the main morphology characteristics and causes were analyzed.A series of measures had been taken through adjustment,op...
Influence of F- on Heat Transfer of Mold Flux and Mineralogical Structure of Flux Film
Zhang Yifei, Han Xiuli, Liu Lei, Liu Lina, Wang Kaiqiang
2016, 37(1): 137-141. doi: 10.7513/j.issn.1004-7638.2016.01.027
Abstract(115) PDF(1)
Abstract:
During continuous casting,the mineralogical structure of flux film and heat transfer of mold flux play important roles in strand quality.In this paper,the thermal conductivity and mineralogical structure of flux film with different F-content were analyzed by the high temperature coefficient of therm...
Study on Hot-rolled Steel Wire Rod for Ultra-high Strength PC Steel Wire and Strand
Hu Lei, Wang Lei, Ma Han
2016, 37(1): 142-147. doi: 10.7513/j.issn.1004-7638.2016.01.028
Abstract(164) PDF(2)
Abstract:
In this paper two hot-rolled steel wire rods for ultra-high strength PC steel wire and strand,i.e.,87A and 90A have been studied by the method of gleeble thermal-mechanical simulation,tensile test,metallographic phase and scanning electron microscopy,the microstructure and mechanical properties of t...
Experimental Study on Softening-melting Properties of Xuanhua Steel BF Iron Burden
Zhao Xiaojie, Liu Ran, Li Haojie
2016, 37(1): 148-152. doi: 10.7513/j.issn.1004-7638.2016.01.029
Abstract(115) PDF(4)
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In this paper softening-dripping experiment was carried out according to Xuanhua Steel blast furnace structure.Single mine drop test results show that the commonly used two kinds of plant of xuanhua steel sinter have good softening performance but poor drop performance where at 1 520℃ it is still dr...
2016, 37(1): 153-154.
Abstract(43) PDF(0)
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