IN SITU SYNTHESIS OF Fe-TiC COMOPOSITES UNDER GREAT THERMAL FLUX
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摘要: 首次应用Gleeble热模拟机研究Fe-Ti-C体系在大热流通量条件下原位合成Fe-TiC复合材料。通过压坯在加热升温过程所反映出的特点,结合热力学计算,以及对产物的X射线衍射分析(XRD)、扫描电镜(SEM)以及能谱分析(EDS)等的研究分析,结果表明:在大热流通量下,可以大幅度地降低合成反应起始温度,且反应完全。在实验研究条件下,Fe-Ti-C体系可在394℃的低温条件下发生合成反应。合成的产物除了分布在铁基体中的小颗粒TiC外,还有少量的Fe2Ti。此研究结果为低温合成Fe-TiC复合材料提供了一条新途径。
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关键词:
- 热流通量 /
- Fe-TiC复合材料 /
- 原位合成 /
- 热力学 /
- 热模拟
Abstract: In situ synthesis of Fe-TiC composites was investigated firstly using Gleeble thermal simulation apparatus under the great thermal flux in the Fe-Ti-C system. A series of studying was taken,such as the temperature feature of compact in the process of heating, the thermodynamic calculation,the analysis of the final product by X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersion spectrometry (EDS). The results show that the starting temperature of synthesis reaction can be decreased greatly. In this study, the synthesis react can take place at a temperature as low as 394℃ in Fe-Ti-C system Besides the litter Particles TiC in Fe-binder phase, there is a little Fe2Ti in the final products. The study provides a new route for producing Fe-TiC composites at low temperature.-
Key words:
- thermal flux /
- Fe-TiC composites /
- in situ synthesis /
- thermodynamics /
- thermal simulation
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